Kersti Vaarmets "Electrochemical and physical characterization of pristine and activated molybdenum carbide - derived carbon electrodes for the oxygen electroreduction reaction"

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View all other units

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Date:

30.06.2014 - 10:00 to 12:00

Thesis supervisors:
Professor Enn Lust, University of Tartu
PhD Jaak Nerut, University of Tartu

Opponent:
Professor Pawel J. Kulesza, University of Warsaw, Poland

Summary:
Alternative energy conversion systems are novel solution for the energy and environmental crisis due to the limited resources of fossil fuels and the globally increasing pollution level. Many countries have invested into development of the environmental friendly renewable-and hydrogen energy technology. Polymer electrolyte membrane fuel cell (PEMFC) is a promising alternative energy conversion system, which has very high electrical efficiency because the energy of the chemical reaction is directly converted into electrical energy. The overall efficiency can be increased even further if the generated heat is used as well.

The electrochemical reactions occur on the surface of the catalyst, which usually is platinum nanoparticles supported onto the porous carbon. To minimize the use of platinum in the catalyst layer and through that the cost of a fuel cell, it is important to design a catalyst structure, which has small Pt-nanoparticles with large effective surface area finely dispersed at the porous surface of the catalyst support.

This is the first systematic study where the molybdenum carbide derived carbons (C(Mo2C)) with tuneable porosity have been studied as a catalyst support for the oxygen electroreduction (ORR). For this work the C(Mo2C)s were prepared from Mo2C at six different fixed chlorination temperatures from 600 °C to 1000 °C and the ORR kinetics was studied on different pristine C(Mo2C) and Pt nanoclusters activated composite Pt-C(Mo2C) and Pt Ru alloy nanoclusters activated Pt-Ru-C(Mo2C) electrode materials in 0.5 M H2SO4 solution at 22 ± 1°C.

It was demonstrated that ORR at micromesoporous carbons strongly depends on the C(Mo2C) synthesis temperature, i.e. on the porosity, pore size distribution, ratio of micropore and mesopore surface area and volume, crystallinity and amount of catalytically active defected areas, expressed at the C(Mo2C) surface.

Location:

Ravila 14a-1021

URL:

hdl.handle.net/10062/41042

Event category:

Defence

M	T	W	T	F	S	S
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8 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	9 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	10 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	11 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	12 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	13 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	14 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral
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22 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	23 103rd anniversary of the Republic of Estonia at the University of Tartu Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	24 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	25 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	26 Tartu International Law Conversations: “Russia's Views on the Regulation of Cyber Operations in International Law” Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	27 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral	28 Graphic art by Katri Smitt in Centre for Arts gallery The Exhibition “The enchanting art of stone cutting. Morgenstern 250” Photo exhibition “Beautiful Youth” in Delta Estonia's National University 100: Photo exhibition “Put on Your Thinking Cap! The Hundred Faces of the University of Tartu” Aarne Maasik’s Photos of Tartu Cathedral

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Kersti Vaarmets "Electrochemical and physical characterization of pristine and activated molybdenum carbide - derived carbon electrodes for the oxygen electroreduction reaction"

February